The synthetic method of 2,6-diformyl-4-methylphenol in a modified Duff reaction is improved. Compared with the literature method, modification for the synthetic method leads to shortened reaction time, simplified operational processes and improved yield.

• 对文献报道的以对甲笨酚为原料.；三氟乙酸为溶剂；利用改进duff反应合成2；6-二甲酰基-4-甲基苯酚的反应过程进行了研究；改进了合成方法；缩短了反应时间；简化了操作步骤；提高了反应产率