The preparation of 3,5-dinitroacetophenone from 3,5-dinitrobenzoic acid and diethyl malonate has been investigated.

• 本文采用丙二酸二乙酯合成法,以3,5-二硝基苯甲酸为原料,经酰化、缩合、脱酸等步骤合成了3,5-二硝基苯乙酮。