Azoisobutyronitrile formamide was prepared by oxidization of hydroazoisobutyronitrile formamide which was synthesized through the reaction of semicarbazide and acetone cyanohydrin.

• 以水合肼和尿素反应制得氨基脲,再与丙酮氰醇反应,经过氧化脱氢合成了偶氮异丁腈甲酰胺。