A method for the determination of 12 organophosphorus pesticide residues(OPs) in red wine by fiber solid phase microextraction(SPME) coupled with gas chromatography(GC) was developed and validated.

• 采用溶胶-凝胶包埋技术制备了耐高温固相微萃取头(SPME),用该萃取头与气相色谱-热离子化检测器联用对红葡萄酒中的12种有机磷农药残留进行了测定。